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Reaction of 6-substituted 3-amino-2-aryl-4(3H)-quinazolinones with D-glucose and D-galactose

Abdo, Mohamed A., Abdel-megeed, Mohamed F., Saleh, Mohamed A. and El-Hiti, Gamal A. 1995. Reaction of 6-substituted 3-amino-2-aryl-4(3H)-quinazolinones with D-glucose and D-galactose. Polish Journal of Chemistry 69 , pp. 583-590.

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Abstract

The reaction of 6-substituted 3-amino-2-aryl-4(3H)-quinazolinones (1-5) with D-glucose and D-galactose in boiling methanol in the presence of acetic acid as a catalyst yielded a mixture of a- and (3-anomers of 6-substituted 2-aryl-3-[N-(D-glycopyranosyl)]-amino-4-(3H)-quinazolinones. The N-glycopyranoside derivatives 6-12 were acetylatcd with acetic anhydride/pyridine to give the corresponding acetates 13-19. Deacetylation of 13, 14, 18, 19 gave 6-substituted 2-aryl-3-[N-acetyl-N-((b-D-glycopyranosyl)]-arnino-4(3II)-quinazolinones (20-23) as sterically hindered exo- and cndoisomcrs.

Item Type: Article
Date Type: Publication
Status: Published
Schools: Chemistry
Subjects: Q Science > QD Chemistry
ISSN: 0137-5083
Last Modified: 19 Mar 2016 22:25
URI: http://orca-mwe.cf.ac.uk/id/eprint/15619

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